| 角鲨烯软胶囊中角鲨烯的鉴定和分析 |
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| 引用本文： | 雷富,许铭本,何小英,张荣灿,姜发军.角鲨烯软胶囊中角鲨烯的鉴定和分析[J].广西科学院学报,2011,27(3):199-201. |
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| 作者姓名： | 雷富 许铭本 何小英 张荣灿 姜发军 |
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| 作者单位： | 广西科学院,广西南宁,530007 |
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| 基金项目： | 广西科学院基本科研业务费项目(编号:09YJ17HY01)资助 |
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| 摘 要： | 用红外光谱和质谱对角鲨烯软胶囊中的角鲨烯进行成分鉴定,用气相色谱-质谱法测定角鲨烯含量。结果表明：所建立的气相色谱-质谱定量分析方法的平均回收率为98.7%,相对标准偏差为5.9%,线性相关系数为0.9999,最低检出限为0.6ng/ml。
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| 关 键 词： | 角鲨烯 气相色谱-质谱 红外光谱 |
| 收稿时间： | 2010/7/23 0:00:00 |
Identification and Analysis of Squalene in Capsule |
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| LEI Fu,XU Ming-ben,He Xiao-ying,ZHANG Rong-can and JIANG Fa-jun.Identification and Analysis of Squalene in Capsule[J].Journal of Guangxi Academy of Sciences,2011,27(3):199-201. |
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| Authors: | LEI Fu XU Ming-ben He Xiao-ying ZHANG Rong-can and JIANG Fa-jun |
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| Institution: | LEI Fu,XU Ming-ben,He Xiao-ying,ZHANG Rong-can,JIANG Fa-jun (Guangxi Academy of Sciences,Nanning,Guangxi,530007,China) |
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| Abstract: | Infrared spectroscopy and mass spectrometry were used to identify squalene in capsule,and the content of squalene was analyzed by gas chromatography-mass spectrometry.Results showed that the average recovery of the quantitative analysis established by gas chromatography-mass spectrometry was 98.7%;the relative standard deviation was 5.9%;linear correlation coefficient was 0.9999;the detection limit was 0.6ng/ml. spectrum |
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| Keywords: | squalene gas chromatography-mass spectrometry infrared |
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