Sulfur ylides 8.* synthesis of 5-methylthio-7,8-dihydro-4,8a-diazfluorene-6,9-dione |
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Authors: | F. Z. Galin S. N. Lakeev L. F. Chertanova G. A. Tolstikov |
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Affiliation: | (1) Institute of Organic Chemistry, Ufa Research Center for Russian Academy of Sciences, 71 prosp. Oktyabrya, 450054 Ufa, Russian Federation |
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Abstract: | Intramolecular cyclization of ketostabilized sulfur ylide obtained from β-alanine and 2,3-pyridinedicarboxylic anhydride was studied. The structure of the reaction product, 5-methylthio-7,8-dihydro-4,8a-diazafluorene-6,9-dione, was established by X-ray diffraction analysis. For Part 7, see Ref. 1. Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 11, pp. 2376–2378, November, 1998. |
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Keywords: | ketostabilized sulfur ylides intramolecular cyclization 5-methylthio-7,8-dihydro-4,8a-diazafluorene-6,9-dione |
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