| The Molecular and Crystal Structure of an Inclusion Compound Formed between Acetylferrocene Pyridine-2, 6-diformylhydrazone and Ethanol |
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| 引用本文： | JI Bao-Ming ,SHEN Yi-Yang (Department of Chemistry,Luoyang Teacher's College,Luoyang 47lO22,P. R. China)WU Yang-Jie, DING Kui-Ling, HUO Shou-Quan (Department of Chemistry,Zhengzhou University,Zhengzhou 450052,P. R. China). The Molecular and Crystal Structure of an Inclusion Compound Formed between Acetylferrocene Pyridine-2, 6-diformylhydrazone and Ethanol[J]. 结构化学, 1998, 0(5) |
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| 作者姓名： | JI Bao-Ming SHEN Yi-Yang (Department of Chemistry Luoyang Teacher's College Luoyang 47lO22 P. R. China)WU Yang-Jie DING Kui-Ling HUO Shou-Quan (Department of Chemistry Zhengzhou University Zhengzhou 450052 P. R. China) |
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| 作者单位： | JI Bao-Ming ;SHEN Yi-Yang (Department of Chemistry，Luoyang Teacher's College，Luoyang 47lO22，P. R. China)WU Yang-Jie; DING Kui-Ling; HUO Shou-Quan (Department of Chemistry，Zhengzhou University，Zhengzhou 450052，P. R. China) |
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| 摘 要： | 1INTR0DUCTI0NIthasbeenreportedthatacety1ferrocenepyridine-2,6-diformylhydrazonewasabletoformbinuclearcomplexeswithrareearthpicratesintheketoforminourpre-viouswork[li.Inthecourseofpurificati0n0fthisligand,wefoundthatitselective1yformsstableinclusi0ncrystalswithethanol.Inordertoelucidatethecoordinationbe-havi0urandtheinclusionpatternofthisligand,themolecularandcrystalstructureofitsinclusioncompoundwithethanolwasreportedinthepresentpaper-2EXPERIMENTAL2.1GeneraIConsiderationTheC,HandNmi…
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The Molecular and Crystal Structure of an Inclusion Compound Formed between Acetylferrocene Pyridine-2, 6-diformylhydrazone and Ethanol |
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| JI Bao-Ming ,SHEN Yi-Yang. The Molecular and Crystal Structure of an Inclusion Compound Formed between Acetylferrocene Pyridine-2, 6-diformylhydrazone and Ethanol[J]. Chinese Journal of Structural Chemistry, 1998, 0(5) |
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| Authors: | JI Bao-Ming SHEN Yi-Yang |
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| Abstract: | : The crystal structure of an inclusion compound formed between acetyl-ferrocene pyridine-2, 6-diformylhydrazone and ethanol was report in the present work.The crystal of C33,H35N5O3Fe2 is monoclinic, space group C2/c with a = 23. 249 (3 ), b=ll. 576(2), c=22. 794(4) A, β=103. 53(l)', V=5964(1) A3, Mr=66l- 37, Z=8, Dc= 1. 473g/cm3, F (000) = 2752. 00, μ = 10. l5 cm-1. It was found that theethanol molecule present in the crystal lattice depends on the van der Waals force ratherthan hydrogen bonding. |
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| Keywords: | ethanol crystal structure acetylferrocene inclusion compound |
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