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Voltammetric Determination of Tin(II) and Iron(II) on Mechanically Renewed Graphite Electrode in Tin-Plating Electrolyte
Authors:Skvortsova  L I  Medvedev  A Zh
Institution:(1) Institute of Solid-State Chemistry and Mechanochemistry, Siberian Division, Russian Academy of Sciences, Novosibirsk, Russia
Abstract:The analytical properties of the cathodic peak of tin(II) reduction and the anodic peak of iron(II) oxidation on a graphite electrode were studied with the electrode surface mechanically renewed directly in a solution before applying a potential in each measurement. The influence of the organic components of the phenolsulfonic tin-plating electrolyte on the cathodic current of tin(II) reduction and anodic current of iron(II) oxidation was studied. A dc voltammetric method was proposed for determining tin(II) directly in the phenolsulfonic tin-plating electrolyte, and iron(II) after the electrolyte is diluted tenfold with a 0.5M H2SO4 supporting solution.
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