| 硫杂杯[4]芳烃酰胺基硫脲衍生物的合成 |
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| 引用本文： | 黄翠玉,杨发福,赵夏,郭红玉,林建荣. 硫杂杯[4]芳烃酰胺基硫脲衍生物的合成[J]. 合成化学, 2006, 14(3): 264-265,268 |
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| 作者姓名： | 黄翠玉 杨发福 赵夏 郭红玉 林建荣 |
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| 作者单位： | 福建师范大学,化学与材料学院,福建,福州,350007;福建师范大学,化学与材料学院,福建,福州,350007;福建师范大学,化学与材料学院,福建,福州,350007;福建师范大学,化学与材料学院,福建,福州,350007;福建师范大学,化学与材料学院,福建,福州,350007 |
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| 基金项目： | 中国科学院资助项目 , 福建省自然科学基金 |
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| 摘 要： | 硫杂杯[4]芳烃四乙酸乙酯衍生物与水合肼反应生成硫杂杯[4]芳烃四酰肼衍生物(3),3与异硫氰酸苯酯反应得到新型硫杂杯[4]芳烃酰胺基硫脲衍生物,总产率61%。
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| 关 键 词： | 硫杂杯[4]芳烃 酰胺 硫脲 合成 |
| 文章编号： | 1005-1511（2006）03-0264-02 |
| 收稿时间： | 2005-12-06 |
| 修稿时间： | 2005-12-06 |
Synthesis of Thiacalix[4]arene Derivatives Containing Amide and Thiourea Units |
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| HUANG Cui-yu,YANG Fa-fu,ZHAO Xia,GUO Hong-yu,LIN Jian-rong. Synthesis of Thiacalix[4]arene Derivatives Containing Amide and Thiourea Units[J]. Chinese Journal of Synthetic Chemistry, 2006, 14(3): 264-265,268 |
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| Authors: | HUANG Cui-yu YANG Fa-fu ZHAO Xia GUO Hong-yu LIN Jian-rong |
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| Affiliation: | College of Chemistry and Materials Science, Fujian Normal University, Fuzhou 350007, China |
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| Abstract: | Thiacalix[4]arene hydrazides derivative(3) was obtained by the reaction of thiacalix[4]arene tetra-ethylacetates with hydrazine hydrate.Treatment of 3 with phenyl isothiocyanate,a novel thiacalix[4]arene derivative containing amide and thiourea units was obtained.The total yield was as high as 61%. |
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| Keywords: | thiacalix[4]arene amide thiourea synthesis |
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