| 铝-碱金属氟化物在超声辐射下于水中诱发的芳香醛还原偶联 |
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| 引用本文： | 李记太,陈艳雪,蔺志平,李同双. 铝-碱金属氟化物在超声辐射下于水中诱发的芳香醛还原偶联[J]. 有机化学, 2005, 25(12): 1583-1586 |
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| 作者姓名： | 李记太 陈艳雪 蔺志平 李同双 |
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| 作者单位： | 河北大学化学与环境科学学院,河北省分析科学技术重点实验室,保定,071002 |
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| 摘 要： | 超声辐射下, 铝粉在氟化钾或氟化钠的水溶液中, 可使芳香醛快速还原或偶联, 生成相应的双分子还原偶联产物和少量单分子还原产物, 其中还原偶联产物邻二醇的收率达15%～82%.
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| 关 键 词： | 超声辐射 还原偶联 邻二醇 合成 |
| 收稿时间： | 2005-01-26 |
| 修稿时间： | 2005-06-06 |
Aluminum/fluoride Salt-mediated Reductive Coupling of Aromatic Aldehydes in Aqueous Media under Ultrasound Irradiation |
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| LI,Ji-Tai,CHEN,Yan-Xue,LIN,Zhi-Ping,LI,Tong-Shuang. Aluminum/fluoride Salt-mediated Reductive Coupling of Aromatic Aldehydes in Aqueous Media under Ultrasound Irradiation[J]. Chinese Journal of Organic Chemistry, 2005, 25(12): 1583-1586 |
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| Authors: | LI Ji-Tai CHEN Yan-Xue LIN Zhi-Ping LI Tong-Shuang |
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| Affiliation: | Key Laboratory of Analytical Science and Technology of Hebei Province, College of Chemistry and Environmental Science, Hebei University, Baoding 071002 |
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| Abstract: | Under ultrasound irradiation, reductive coupling of aromatic aldehydes mediated by A1/KF or NaF in aqueous media afforded 1,2-diol in 15%-82% yields. |
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| Keywords: | ultrasound irradiation reductive coupling 1 2-diol synthesis |
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