| 基于宽表面等离子体吸收带纳米银膜的制备及其SERS活性研究 |
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| 引用本文： | 张德清,司民真,刘仁明,柳振全. 基于宽表面等离子体吸收带纳米银膜的制备及其SERS活性研究[J]. 光谱学与光谱分析, 2012, 32(9): 2438-2441. DOI: 10.3964/j.issn.1000-0593(2012)09-2438-04 |
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| 作者姓名： | 张德清 司民真 刘仁明 柳振全 |
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| 作者单位： | 楚雄师范学院物理与电子信息系光谱技术应用研究所，云南 楚雄 675000 |
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| 基金项目： | 国家自然科学基金项目，云南省基金项目，楚雄师范学院学术后备人才项目 |
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| 摘 要： | 在恒温条件下，采用静电自组装技术在玻璃表面制备了一种具有宽等离子吸收带的纳米银膜。使用扫描电镜(SEM)观察其表面形貌发现该纳米银膜表面由粒径为18～200 nm的纳米球组成。同时从紫外可见光谱检测结果发现该纳米银膜在400～850 nm间有较宽的等离子吸收带。分别以强荧光分子(结晶紫)和生物大分子(健康人血清)作为探针分子，在近红外激发光(785 nm)下检测出了质量较好的SERS光谱。同时，分析了该纳米银膜对两种分子检测的重复性。
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| 关 键 词： | 恒温 表面增强拉曼散射 纳米银膜 血清 表面等离子体共振 |
| 收稿时间： | 2012-02-28 |
Preparation and SERS Activity Studies on Substrate of Nano-Silver Film with Broad Plasma Absorption Band |
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| ZHANG De-qing , SI Min-zhen , LIU Ren-ming , LIU Zhen-quan. Preparation and SERS Activity Studies on Substrate of Nano-Silver Film with Broad Plasma Absorption Band[J]. Spectroscopy and Spectral Analysis, 2012, 32(9): 2438-2441. DOI: 10.3964/j.issn.1000-0593(2012)09-2438-04 |
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| Authors: | ZHANG De-qing SI Min-zhen LIU Ren-ming LIU Zhen-quan |
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| Affiliation: | Department of Physics and Electronic Science, Chuxiong Normal University, Chuxiong 675000, China |
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| Abstract: | A highly reproducible and broad plasma absorption band nano-silver film was prepared by electrostatic self-assembly technology.The size of nano-silver particles on the surface of silver film,in the scanning electron microscopy(SEM) micrograph,is in a wide distribution from 18 to 200 nm.At the same time,the ultraviolet-visible spectrophotometer was employed to detect the nano-silver film.There is a broad plasma absorption band in the UV-Vis spectrum.To test the SERS activity of the nano-silver film,crystal violet and serum of healthy person were used as probe molecules and the high quality SERS spectra were obtained. |
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| Keywords: | Constant temperature SERS,Nano-silver film Serum SPR |
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