| STRUCTURE OF 1-PHENYL-3,4-BENZO-7,10-DIMETHYL-2,8,9-TRIOXA-5-A2A- SILATRICYCLO(3.3.3.0~(1,5))UNDECANE |
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| 摘 要： | <正> Mr=327.49, monoclinic,C2/c,a=17.211(11), b=12.300(7),c=17.079(10)A,β=99.41(5)°,V=3567(4)A3,Z=8,μ(MoKα)=1.5cm-1,F(000)=1392,Dx=1.22g/cm3, room temperature.The final R=0.085,Rw=0.077 and s=1.27 for 1471 independent reflections with |Fo|>2.5σ(|Fo|).The length of the dative bond N→Si is 2.193(5)A.The structure Is disordered at C(7),C(13),C(10), C(12)positions.
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STRUCTURE OF 1-PHENYL-3,4-BENZO-7,10-DIMETHYL-2,8,9-TRIOXA-5-A2A- SILATRICYCLO(3.3.3.0(1,5))UNDECANE |
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| Abstract: | Mr=327.49, monoclinic,C2/c,a=17.211(11), b=12.300(7),c=17.079(10)A,β=99.41(5)°,V=3567(4)A3,Z=8,μ(MoKα)=1.5cm-1,F(000)=1392,Dx=1.22g/cm3, room temperature.The final R=0.085,Rw=0.077 and s=1.27 for 1471 independent reflections with |Fo|>2.5σ(|Fo|).The length of the dative bond N→Si is 2.193(5)A.The structure Is disordered at C(7),C(13),C(10), C(12)positions. |
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