New 12-tungstophosphate-based organic-inorganic hybrid. Synthesis, spectroscopic characterization, X-ray determination and thermal behavior |
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| Authors: | M. Pourayoubi A. R. Mahjoub F. Maleki S. Ghammamy P. Lavaee |
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| Affiliation: | 1. Department of Chemistry, Tarbiat Modares University, Tehran, Iran
2. Department of Chemistry, Faculty of Sciences, Imam Khomeini International University, Qazvin, Iran
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| Abstract: | 12-Tungstophosphate-based organic/inorganic hybrid, [HNMPA]3[O40PW12].0.5NMPA.2H2O (NMPA = N-methylpropionamide) was synthesized and characterized by IR, UV-Vis, 1H, 13C and 31P NMR spectroscopies, elemental analysis, TGA, DTA and single crystal X-ray determination. Full decomposition of the hybrid leads to WO3 powder was studied by IR, SEM and XRD. |
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