One-pot three-component reaction of C60, amino acid and fluorinated benzaldehyde to C60-pyrrolidine derivatives |
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| Authors: | Sheng Wang Li-ping Song Hu Jiang |
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| Institution: | a Department of Chemistry, School of Science, Shanghai University, No. 99 Shangda Road, Shanghai 200436, China
b State Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Science, Shanghai 200032, China |
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| Abstract: | A series of fluorinated 2,5-disubstituted C60-pyrrolidine derivatives were synthesized via one-pot three-component reaction of C60, amino acid and fluorinated benzaldehyde under reflux in toluene or microwave irradiation. The cis- and trans-isomers could be isolated by chromatography and fully confirmed by 1H NMR. |
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| Keywords: | C60 Amino acid Fluorinated benzaldehyde 1 3-Dipolar cycloaddition C60-pyrrolidines |
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