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The structure of the proton skeleton in 1,3-butadieneiron Tricarbonyl as determined from the NMR spectra of oriented molecules
Authors:P. Diehl  A.C. Kunwar  H. Zimmermann
Affiliation:Department of Physics and Physical Chemistry, University of Basel, 82, Klingelbergstrasse, CH 4056 Basel Switzerland
Abstract:1H NMR spectra of 1,3-butadieneiron tricarbonyl oriented in a nematic liquid crystal solvent have been analysed and used to derive the structure of the proton skeleton, which is found to be non-planar. The distance of the anti protons from the plane defined by the remaining four protons is 0.77 ± 0.06 ±.
Keywords:To whom correspondence should be sent at his present address: Sterling Chemistry Laboratory. Yale University   225 Prospect Street   New Haven   Conn. 06520 (U.S.A.).
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