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A green protocol for catalyst-free synthesis of 1-oxo-hexahydroxanthenes in aqueous medium
Authors:DM Pore  TS Shaikh  KA Undale  DS Gaikwad
Institution:a Department of Chemistry, Shivaji University, Kolhapur 416 004, India
Abstract:An efficient and eco-friendly synthesis of 1-oxo-hexahydroxanthenes has been expediently accomplished by a reaction of salicylaldehyde with cyclohexane-1,3-dione or dimedone in water as universal solvent at reflux condition without a catalyst. Excellent yields of the products, operational simplicity, simple work-up and catalyst-free synthesis are attractive features of this green protocol.
Keywords:Octahydroxanthene  Hexahydroxanthene  Salicylaldehyde  Water  Cyclohexane-1  3-dione  Dimedone
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