An apparatus for the determination of speeds of sound in fluids

An apparatus for accurate measurements of the sound velocity in fluids is described, which is based on the pulse-echo technique, and operates up to 30 MPa in the temperature range between (250 and 350) K. The expanded uncertainties (k = 2) in the speed of sound measurements are 0.006%, 6 mK in the temperature, 2.1 hPa in the pressure up to 3 MPa, and 23.9 hPa above this value. Measurements of the speed of sound for nitrogen from (250 to 350) K and for water at temperatures between (303.15 and 323.15) K are presented at pressures up to 30 MPa to validate the new apparatus. The expanded overall uncertainty of the measurements on nitrogen and water were estimated to be 0.011% and 0.006%, respectively. The speed of sound of both fluids was compared with literature sources showing an excellent agreement among them, with relative deviations lower than 0.01% in nitrogen and 0.006% in water.