| 快速石墨炉原子吸收法测定地面水中痕量铜和铅 |
| |
| 引用本文： | 郁建桥,陈素兰,刘建琳.快速石墨炉原子吸收法测定地面水中痕量铜和铅[J].光谱学与光谱分析,2000,20(4):547-549. |
| |
| 作者姓名： | 郁建桥 陈素兰 刘建琳 |
| |
| 作者单位： | 江苏省环境监测中心,210029,南京 |
| |
| 摘 要： | 本文探讨了用快速石墨炉原子吸收法测定地面水中痕量铜和铅。系统地研究了石墨炉升温程序及基体改进剂对测定的影响。提出了删去灰化步骤 ,在不需要基体改进剂情况下快速测定环境清洁地面水中铜和铅的方法。铜和铅的方法检出限分别为 0 9μg·L- 1 和 1 2 μg·L- 1 。相对标准偏差 (RSD) (n =1 )分别为 2 5 %和 4 1 %,加标回收率分别在 96 0 %～ 97 2 %和 90 0 %～ 92 0 %之间。
|
| 关 键 词： | 原子吸收法 地面水 铜 铅 痕量分析 环境监测 |
A Rapid Graphite Furnace Atomic Absorption Spectrometric Method for the Determination of Trace Copper and Lead in Surface Water |
| |
| Jianqiao YU,Sulan CHEN,Jianlin LIU.A Rapid Graphite Furnace Atomic Absorption Spectrometric Method for the Determination of Trace Copper and Lead in Surface Water[J].Spectroscopy and Spectral Analysis,2000,20(4):547-549. |
| |
| Authors: | Jianqiao YU Sulan CHEN Jianlin LIU |
| |
| Institution: | Jiangsu Province Environmental Monitoring Center, 210029 Nanjing. |
| |
| Abstract: | A rapid graphite furnace atomic absorption spectrometric method for the determination of trace copper and lead in surface water is investigated in this paper. The influences of the program for graphite furnace and matrix modifier are systematically researched. A rapid method without ashing step and chemical matrix modifier is established. The determination limits of copper and lead are 0.9 microgram.L and 1.2 micrograms.L, respectively. The relatively standard deviations (RSD) (n = 1) are 2.5% and 4.1%, respectively. The recoveries are 96.0%-97.2% and 90.0%-92.0%, respectively. |
| |
| Keywords: | Rapid graphite furnace atomic absorption spectrometry Surface water Copper Lead |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
