| 新型溴乙酰四胺化合物的合成 |
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| 引用本文： | 陈中祝,吕梦岚,张文睿,邓金根,朱槿. 新型溴乙酰四胺化合物的合成[J]. 合成化学, 2011, 19(6): 785-787 |
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| 作者姓名： | 陈中祝 吕梦岚 张文睿 邓金根 朱槿 |
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| 作者单位： | 1. 中国科学院成都有机化学研究所,四川成都610041;中国科学院研究生院,北京100049
2. 中国科学院成都有机化学研究所,四川成都,610041 |
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| 基金项目： | 国家自然科学基金资助项目(21072187) |
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| 摘 要： | 以四胺盐酸盐和2-溴乙酰溴为起始原料,在碳酸钾和二氯甲烷/水中通过缩合反应合成了两个新型溴乙酰四胺化合物,其结构经1H NMR和MS表征.
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| 关 键 词： | 四胺 2-溴乙酰溴 溴乙酰四胺 合成 |
Synthesis of Novel Bromoacetyl Tetramines |
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| CHEN Zhong-zhu,Lü Meng-lan,ZHANG Wen-rui,DENG jin-gen,ZHU Jin. Synthesis of Novel Bromoacetyl Tetramines[J]. Chinese Journal of Synthetic Chemistry, 2011, 19(6): 785-787 |
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| Authors: | CHEN Zhong-zhu Lü Meng-lan ZHANG Wen-rui DENG jin-gen ZHU Jin |
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| Affiliation: | CHEN Zhong-zhu1,2,Lü Meng-lan1,ZHANG Wen-rui1,DENG jin-gen1,ZHU Jin1(1.Chengdu Institute of Organic Chemistry,Chinese Academy of Sciences,Chengdu 610041,China,2.Graduated School of Chinese Academy of Sciences,Beijing 100039,China) |
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| Abstract: | Two novel bromoacetyl tetramines were synthesized by the condensation reaction of tetramine with 2-bromoacetyl bromide in the presence of K2CO3 in solution of CH2Cl2 and H2O.The structures were characterized by 1H NMR and MS. |
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| Keywords: | tetramine 2-bromoacetyl bromide bromoacetyl tetramine synthesis |
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