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| 新型杯[4]芳烃酰肼基羰基羧酸衍生物的合成 | |
| 引用本文： | 刘志强,洪碧琼,杨发福,许冰婷,谢剑伟.新型杯[4]芳烃酰肼基羰基羧酸衍生物的合成[J].合成化学,2011,19(6):775-777. |
| 作者姓名： | 刘志强 洪碧琼 杨发福 许冰婷 谢剑伟 |
| 作者单位： | 1. 福建师范大学化学与材料学院,福建福州,350007 2. 中国人民武装警察部队福州指挥学院教研部,福建福州,350002 3. 福建师范大学化学与材料学院,福建福州350007;福建师范大学福建省高分子材料重点实验室,福建福州350007 |
| 基金项目： | 福建省自然科学基金资助项目(2011J01031); 福建省高校杰出青年科研人才培育计划资助项目(JA10056); 福建省教育厅重点项目(SA11044) |
| 摘 要： | 杯4]芳烃经醚化引入酯基后再经水合肼肼解,进一步与丁二酸酐或顺丁烯二酸酐氨解开环合成了两个新型的杯4]芳烃酰肼基羰基羧酸衍生物,产率85％和83％,其结构经1H NMR,IR和ESI-MS表征. |
| 关 键 词： | 杯[4]芳烃 酰肼 羧酸 合成 |
Synthesis of Novel Calix[4]-hydrazinylcarbonyl Carboxylic Acid Derivatives |
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| LIU Zhi-qiang,HONG Bi-qiong,YANG Fa-fu,XU Bing-ting,XIE Jian-wei.Synthesis of Novel Calix[4]-hydrazinylcarbonyl Carboxylic Acid Derivatives[J].Chinese Journal of Synthetic Chemistry,2011,19(6):775-777. | |
| Authors: | LIU Zhi-qiang HONG Bi-qiong YANG Fa-fu XU Bing-ting XIE Jian-wei |
| Institution: | LIU Zhi-qiang1a,HONG Bi-qiong2,YANG Fa-fu1a,1b,XU Bing-ting1a,XIE Jian-wei1a(a.College of Chemistry and Materials Science,b.Fujian Key Laboratory of Polymer Materials,1.Fujian Normal University,Fuzhou 350007,China,2.Command Academy of Fuzhou,The Chinese People's Armed Police Force,Fuzhou 350002,China) |
| Abstract: | Two novel calix4]-hydrazinylcarbonyl carboxylic acid derivatives in yields of 85% and 83% were synthesized by introducing ester groups into calix4]arene,subsequently ammonolysis with hydrazine hydrate,and then ring-opening reaction with succinic anhydride or maleic anhydride.Their structures were characterized by 1H NMR,IR and ESI-MS. |
| Keywords: | calix[4]arene hydrazide carboxylic acid synthesis |
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