| 反相微乳液法合成钛酸钡纳米棒 |
| |
| 引用本文： | 朱启安,宋方平,陈万平,王树峰,孙旭峰,张琪.反相微乳液法合成钛酸钡纳米棒[J].高等学校化学学报,2006,27(9):1612-1614. |
| |
| 作者姓名： | 朱启安 宋方平 陈万平 王树峰 孙旭峰 张琪 |
| |
| 作者单位： | 湘潭大学化学学院,湘潭 411105 |
| |
| 基金项目： | 国家自然科学基金(批准号:50472080)资助 |
| |
| 摘 要： | 本文在W/O型反相微乳液(Reverse Microemulsion)体系中制得了BaTiO3纳米棒, 考察了ωo值、反应物浓度等因素对BaTiO3纳米棒尺寸及形貌的影响. 用TEM、XRD和电子衍射对材料进行了表征,并用ICP测试了产品中钡与钛的摩尔比.
|
| 关 键 词： | W/O微乳液 BaTiO3 纳米棒 合成 |
| 文章编号： | 0251-0790（2006）09-1612-03 |
| 收稿时间： | 01 6 2006 12:00AM |
| 修稿时间： | 2006-01-06 |
Synthesis of BaTiO3 Nanorods by Reverse Microemulsion Method |
| |
| ZHU Qi-An,SONG Fang-Ping,CHEN Wan-Ping,WANG Shu-Feng,SUN Xu-Feng,ZHANG Qi.Synthesis of BaTiO3 Nanorods by Reverse Microemulsion Method[J].Chemical Research In Chinese Universities,2006,27(9):1612-1614. |
| |
| Authors: | ZHU Qi-An SONG Fang-Ping CHEN Wan-Ping WANG Shu-Feng SUN Xu-Feng ZHANG Qi |
| |
| Institution: | College of Chemistry, Xiangtan University, Xiangtan 411105, China |
| |
| Abstract: | BaTiO3 nanorods were synthesized in water/OP-10/n-hexanol/cyclohexane quaternary reverse microemulsion solution at 60 ℃. The effects of the molar ratio of water to surfactant and the concentration of reactants on the diameters and lengths of BaTiO3 nanorods were studied. The products were characterized by TEM, XRD and ICP. The results show that the diameters and lengths of the prepared BaTiO3 nanorods with a cubic phase and a single crystal are approximately 15~80 nm and 300~3 900 nm, respectively. And the molar ratio of barium to titanium of products is 1.0. |
| |
| Keywords: | W/O microemulsion Barium titanate Nanorods Synthesis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
| 点击此处可从《高等学校化学学报》浏览原始摘要信息 |
| 点击此处可从《高等学校化学学报》下载免费的PDF全文 |
|
