| 微波消解-分光光度法测定大豆中的硼量 |
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| 引用本文： | 徐玉宏. 微波消解-分光光度法测定大豆中的硼量[J]. 分析试验室, 2008, 27(3): 112-114 |
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| 作者姓名： | 徐玉宏 |
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| 作者单位： | 阜阳市环境保护监测站,阜阳,236033 |
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| 摘 要： | 研究了分光光度法测定大豆中的硼时样品的微波消解方法。建立了合理的分析步骤。进行了微波消解条件的选择及方法的精密度、准确度试验。试验结果表明:消解完全仅需20 min,相对标准偏差均小于7.6%,其方法的加标回收率为92%~105%。
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| 关 键 词： | 大豆 微波消解 分光光度法 硼 |
| 文章编号： | 1000-0720（2008）03-112-03 |
| 收稿时间： | 2007-01-06 |
| 修稿时间： | 2007-03-21 |
Determination of boron in soybean by microwave digestion-spectrophotometry |
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| XU Yu-hong. Determination of boron in soybean by microwave digestion-spectrophotometry[J]. Chinese Journal of Analysis Laboratory, 2008, 27(3): 112-114 |
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| Authors: | XU Yu-hong |
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| Abstract: | A method for the determination of boron in soybean samples by spectrophotometry with microwave digestion was proposed. The experimental conditions were optimized. It was found that the samples were digested completely in 20 min by microwave heating. RSD caculated from the 6 determination results for each sample was less than 7.6%.Recoveries were 92% - 105%. The method is rapid, accurate and less polluting. |
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| Keywords: | Soybean Microwave digestion Spectrophotometry Boron |
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