| 反应条件对水热合成二硫化镍NiS2粉晶的影响 |
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| 引用本文： | 蒋莉,郑毓峰,孙言飞,陈艳华,张玲.反应条件对水热合成二硫化镍NiS2粉晶的影响[J].新疆大学学报(理工版),2006,23(4):428-431. |
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| 作者姓名： | 蒋莉 郑毓峰 孙言飞 陈艳华 张玲 |
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| 作者单位： | 新疆大学物理科学与技术学院 乌鲁木齐830046 |
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| 摘 要： | 本文采用水热法一步合成了二硫化镍粉晶,利用X射线衍射(XRD),扫描电子显微镜讨论了样品N iS2粉晶的晶体结构及形貌,研究了X射线衍射峰积分强度以及半峰宽等随反应条件的变化,并分析了N iS2粉晶的合成机理.
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| 关 键 词： | 二硫化镍(NiS_2) 水热法 XRD |
| 文章编号： | 1000-2839（2006）04-0428-04 |
| 收稿时间： | 2006-06-18 |
| 修稿时间： | 2006年6月18日 |
Influence of the Reaction Condition on Synthesizing NiS2 Powder by Hydrothermal Technique |
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| JIANG Li,ZHENG Yu-feng,SUN Yan-fei,CHEN Yan-hua,ZHANG Ling.Influence of the Reaction Condition on Synthesizing NiS2 Powder by Hydrothermal Technique[J].Journal of Xinjiang University(Science & Engineering),2006,23(4):428-431. |
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| Authors: | JIANG Li ZHENG Yu-feng SUN Yan-fei CHEN Yan-hua ZHANG Ling |
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| Institution: | College of Physical Science and Technology, Xinjiang University, Urumqi, Xinjiang 830046, China |
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| Abstract: | NiS_2 Powder has been synthesized through the hydrothermal technique in this paper.Structures and morphology of the final products were characterized with X-ray powder diffraction(XRD),scanning election microscopy(SEM).The integral intensities of XRD peaks as well as measured full width half maximum(FWHM) was stuied with the reaction condition varied and the mechanism of hydrothermal process was analysed. |
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| Keywords: | NiS_2 hydrothermal XRD |
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