Preparation of PbO nanocrystals via decomposition of lead oxalate |
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| Authors: | Masoud Salavati-Niasari Fatemeh Mohandes Fatemeh Davar |
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| Affiliation: | 1. Department of Chemistry, Faculty of Science, University of Kashan, Kashan, P.O. Box 87317-51167, Islamic Republic of Iran;2. Institute of Nano Science and Nano Technology, University of Kashan, Kashan, P.O. Box 87317-51167, Islamic Republic of Iran |
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| Abstract: | The present study reports the preparation and characterization of PbO nanocrystals obtained via a thermal decomposition route. The PbO nanocrystals were synthesized using lead oxalate powder as a precursor. Nanostructured products were investigated by means of XRD, TEM, FT-IR and XPS. The XRD results indicate that tetragonal phase β-PbO with a particle size of about 30–45 nm was obtained when the intermediate precipitate was calcined at 500 °C. |
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| Keywords: | PbO nanocrystals Thermal decomposition Inorganic materials Chemical synthesis |
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