| 甲基二甲氧基硅烷的合成研究 |
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| 引用本文： | 胡碧茹 宋永才. 甲基二甲氧基硅烷的合成研究[J]. 合成化学, 1998, 6(4): 445-448 |
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| 作者姓名： | 胡碧茹 宋永才 |
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| 作者单位： | 国防科学技术大学材料工程与应用化学系 |
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| 摘 要： | 以ＭｅＳｉＨＣｌ２和ＭｅＯＨ为原料，采用溶剂法合成甲基二氧基硅烷，研究了各种合成条件对醇解反应的影响，运用ＩＲ，ＧＣ－ＭＳ等手段对反应过程和结果进行了综合分析，提出了最佳合成条件。
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| 关 键 词： | 甲基二甲氧基 硅烷 醇解反应 溶剂法 合成 |
The Synthesis of Methyldimethoxysilane |
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| Hu,Bi Ru Song,Yong Cai Feng,Chun Xiang. The Synthesis of Methyldimethoxysilane[J]. Chinese Journal of Synthetic Chemistry, 1998, 6(4): 445-448 |
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| Authors: | Hu Bi Ru Song Yong Cai Feng Chun Xiang |
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| Abstract: | Methyldimethoxysilane was synthesized using MeSiHCl 2 and MeOH as starting material in an inert solvent. The effects of reaction conditions on the alcoholysis were studied.The reaction process and composition of products were examined by IR and GC MS method. The appropriate reaction conditions were established. |
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| Keywords: | Methyldimethoxysilane MeSiHCl 2 MeOH Alcoholysis Solvent method Synthesis. |
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