Variants of the complete synthesis of d,l-estrone from 1-vinyl-6-methoxytetralol and 2-methylcyclopentane-1,3-dione |
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| Authors: | K K Koshoev S N Ananchenko and I V Torgov |
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| Institution: | (1) Institute of the Chemistry of Natural Compounds AS USSR, USSR |
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| Abstract: | Summary Various routes for the synthesis of the methyl ether of d,l-estrone (XI) and of d,l-estrone itself (XIII) have been investigated. The best results were obtained by synthesis according to the route IV  V VI I X XI XIII, when the yield of the methyl ether of d,l-estrone (XI) was 25% and that of d,l-estrone 13%, calculated on the basis of 6-methoxytetralone.Khimiya Prirodnykh Soedinenii, Vol. 1, No. 3, pp. 172–180, 1965 |
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