Structural, Spectroscopic, and Thermal Behaviour of Bis -(thiosaccharinate)-aqua-cadmium(II) |
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| Authors: | Susana H Tarulli Oscar V Quinzani Oscar E Piro Enrique J Baran and Eduardo E Castellano |
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| Institution: | (1) Department of General and Coordination Chemistry, Faculty of Chemistry, Maria Curie-Sklodowska University, 20-031 Lublin, Poland; |
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| Abstract: | The crystal structure of the title complex, Cd(tsac)2(H2O)], has been determined by single crystal X-ray diffraction methods. It crystallizes in the monoclinic space group C2/c (a = 12.236(3), b = 8.919(3), c = 16.655(3) ?, β = 96.18(2)°, Z = 4). The molecular structure was solved from 1705 independent reflections with I > σ(I) and refined to R 1 = 0.0489. Infrared and Raman spectra of the complex were recorded and are briefly discussed. Its thermal behaviour was investigated by thermogravimetry and differential thermal analysis. |
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