Preparation and properties characterization of gallic acid epoxy resin/succinic anhydride bionanocomposites modified by green reduced graphene oxide |
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Authors: | Guixiang Hou Jungang Gao Jianqiang Xie Bo Li |
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Affiliation: | 1. Hebei Provincial Key Laboratory of Inorganic Nonmetallic Materials, College of Materials Science and Engineering, North China University of Science and Technology, Tangshan Hebei, Chinahougx2016@126.com;3. College of Chemistry and Environmental Science, Hebei University, Baoding Hebei, China;4. Hebei Provincial Key Laboratory of Inorganic Nonmetallic Materials, College of Materials Science and Engineering, North China University of Science and Technology, Tangshan Hebei, China |
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Abstract: | Graphene oxide was reduced into reducing-graphene oxide (r-GO) successfully using gallic acid (GA) as a green reducing agent. Biobased gallic acid epoxy resin (GAER) was synthesized from renewable GA, and the biobased GAER/r-GO nanocomposites and glass fiber-reinforced composites were prepared with succinic anhydride as a curing agent. The dynamic mechanical, thermal, and mechanical properties of the composites with varying r-GO contents were characterized. When the content of r-GO was 0.5 wt%, the glass transition temperature was 10.4°C higher than the pure resin system. The thermal and mechanical properties were increased with increasing r-GO content; when the r-GO content was 1.0 wt%, the initial degradation temperature was enhanced by approximately 6.8°C, the tensile and impact strengths were 34.5% and 49.1% higher, respectively, than the pure cured GAER. The impact strength of GAER was higher than that of the bisphenol A epoxy resin/SUA curing system, but the tensile strength was lower than it. |
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Keywords: | Gallic acid epoxy resin succinic anhydride graphene green reduction bionanocomposites |
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