Synthesis of 1,3,4-oxadiazoles from 1,2-diacylhydrazines using [Et2NSF2]BF4 as a practical cyclodehydration agent |
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Authors: | Pouliot Marie-France Angers Laetitia Hamel Jean-Denys Paquin Jean-François |
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Institution: | Department of Chemistry, Université Laval, Québec, Canada. |
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Abstract: | The preparation of 1,3,4-oxadiazoles from 1,2-diacylhydrazines using XtalFluor-E (Et(2)NSF(2)]BF(4)) as cyclodehydration reagent is described. Various functionalized 1,3,4-oxadiazoles were synthesized and it was found that the use of acetic acid as an additive generally improved the yields. |
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