| Synthesis and Crystal Structure of 4-Bromo-5-ethoxy-3-methyl-5- （naphthalen- 1-yl）- 1-tosyl- 1H-pyrrol-2（5H）- one |
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| 作者姓名： | SHEN Ru-Wei YANG Yu-Zhu CAO Jian WU Lu-Ling HUANG Xian |
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| 作者单位： | Department of Chemistry, Zhejiang University （Xixi Campus）, Hangzhou 310028, China |
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| 摘 要： | The title compound 4-bromo-5-ethoxy-3-methyl-5-(naphthalen-1-yl)-1-tosyl-1H- pyrrol-2(5H)-one 1 (C24H22BrNO4S, Mr = 500.40) has been synthesized and its crystal structure was determined by single-crystal X-ray diffraction analysis. It crystallizes in monoclinic, space group P21/n with a = 8.8562(15), b = 18.118(3), c = 14.055(2) , β = 99.855(3)o, V = 2221.9(6) 3, Z = 4, Dc = 1.496 g/cm3, μ = 1.975 mm-1, λ = 0.71073 , F(000) = 1024, R = 0.0607 and wR = 0.1371.
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| 关 键 词： | 乙氧基 甲基 甲苯磺酰基 晶体结构 |
| 收稿时间： | 2007-01-23 |
| 修稿时间： | 2007-04-16 |
Synthesis and Crystal Structure of 4-Bromo-5-ethoxy-3-methyl-5-(naphthalen-1-yl)-1-tosyl-1H-pyrrol-2(5H)-one |
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| SHEN Ru-Wei YANG Yu-Zhu CAO Jian WU Lu-Ling HUANG Xian.Synthesis and Crystal Structure of 4-Bromo-5-ethoxy-3-methyl-5-(naphthalen-1-yl)-1-tosyl-1H-pyrrol-2(5H)-one[J].Chinese Journal of Structural Chemistry,2007,26(12):1505-1508. |
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| Authors: | SHEN Ru-Wei YANG Yu-Zhu CAO Jian WU Lu-Ling HUANG Xian |
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| Abstract: | The title compound 4-bromo-5-ethoxy-3-methyl-5-(naphthalen-1-yl)-1-tosyl-1H-pyrrol-2(5H)-one 1 (C24H22BrNO4S, Mr = 500.40) has been synthesized and its crystal structure was determined by single-crystal X-ray diffraction analysis. It crystallizes in monoclinic, space group P21/n with a = 8.8562(15), b = 18.118(3), c = 14.055(2)(A), β = 99.855(3)°, V = 2221.9(6)(A)3, Z= 4, Dc = 1.496 g/cm3, μ = 1.975 mm-1, λ = 0.71073 (A), F(000) = 1024, R = 0.0607 and wR= 0.1371. |
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| Keywords: | 4-bromo-5-ethoxy-3-methyl-5-(naphthalen-1-yl)-1-tosyl-1H-pyrrol-2(5H)-one synthesis crystal structure Crystal Structure space group synthesized crystal structure diffraction analysis compound |
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