| 二苄基锡双(吗啉荒酸酯)的合成、表征及晶体结构 |
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| 引用本文： | 尹汉东,王传华,王勇,张如芬,马春林. 二苄基锡双(吗啉荒酸酯)的合成、表征及晶体结构[J]. 无机化学学报, 2002, 18(2): 201-204 |
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| 作者姓名： | 尹汉东 王传华 王勇 张如芬 马春林 |
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| 作者单位： | 聊城师范学院化学系,聊城,252059 |
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| 基金项目： | 教育部骨干教师基金，山东省自然科学基金资助项目(No.Y2000B08) |
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| 摘 要： | Dibenzyltin bis(dithiomorpholinocarbamate) was synthesized by the reaction of dibenzyltin dichloride with dithiomorpholinocarbamate. The compound was characterized by elemental analysis, IR, 1H NMR and MS. and the crystal structure was determined by X-ray single crystal diffraction. The crystal belongs to orthorhombic with space group Pca21, a=1.8327(3)nm, b= 0.65678(12)nm, c=2.2583(4)nm, Z=4, V=2.718 (9)nm3, Dx=1.528g·cm-3,μ=1.271mm-1, F(000)=1272, R1=0.0434, wR2=0.1152. In the crystals, the structures consist of discrete molecules containing six-coordinate tin atoms in a distorted octahedron configuration.
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| 关 键 词： | 二苄基锡吗啉荒酸酯 合成 晶体结构 |
| 修稿时间： | 2001-06-11 |
Synthesis, Characterization and Crystal Structure of Dibenzyltin Bis(Dithiomorpholinocarbamate) |
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| YIN Han-Dong,WANG Chuan-Hu,WANG Yong,ZHANG Ru-Fen and MA Chun-Lin. Synthesis, Characterization and Crystal Structure of Dibenzyltin Bis(Dithiomorpholinocarbamate)[J]. Chinese Journal of Inorganic Chemistry, 2002, 18(2): 201-204 |
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| Authors: | YIN Han-Dong WANG Chuan-Hu WANG Yong ZHANG Ru-Fen MA Chun-Lin |
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| Affiliation: | Department of Chemistry, Liaocheng Teachers University, Liaocheng 252059,Department of Chemistry, Liaocheng Teachers University, Liaocheng 252059,Department of Chemistry, Liaocheng Teachers University, Liaocheng 252059,Department of Chemistry, Liaocheng Teachers University, Liaocheng 252059 and Department of Chemistry, Liaocheng Teachers University, Liaocheng 252059 |
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| Abstract: | |
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| Keywords: | dibenzyltin dithiomorpholinocarbamate synthesis crystal structure |
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