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Determination of persistent organohalogenated pollutants in human hair reference material (BCR 397): an interlaboratory study
Authors:Udai Gill  Adrian Covaci  John Jake Ryan  Andre Emond
Institution:(1) Product Safety Laboratory, Health Canada, Ottawa, Ontario K1A0L2, Canada;(2) Toxicological Center, University of Antwerp, Universiteitsplein 1, 2610 Wilrijk, Belgium;(3) Bureau of Chemical Safety, Health Products and Food Branch, Health Canada, Ottawa, Ontario K1A0L2, Canada;(4) Environmental Research Division, First Nations and Inuit Health Branch, Health Canada, Ottawa, Ontario K1A0L2, Canada
Abstract:A human powdered hair material (BCR 397) was tested for its content in persistent organic pollutants (POPs), such as polychlorinated biphenyls (PCBs), organochlorine pesticides (OCPs) and polybrominated diphenyl ethers (PBDEs). Using different methods, three laboratories (two from Canada and one from Belgium) analysed a powdered hair sample to evaluate some methodologies and to obtain consensus values for selected POPs. Measured values for all PCB congeners and p,pprime-DDE were within a relative standard deviation (RSD) of 15%. These first results contribute to the accuracy and precision for POPs quantification in hair and render test results more comparable among different laboratories.
Keywords:Polychlorinated biphenyls  Organochlorine pesticides  Polybrominated diphenyl ethers  Human hair  BCR 397  Interlaboratory study
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