Tosylation of endocrine-disruptive alkylphenolic compounds in a solid-phase reaction system consisting of C18-modified silica gel and aqueous buffer solution |
| |
Authors: | Uno Bunji Okumura Noriko |
| |
Affiliation: | Gifu Pharmaceutical University, Mitahora-higashi, Gifu, Japan. uno@gifu-pu.ac.jp |
| |
Abstract: | The tosylation reaction of endocrine-disruptive alkylphenolic compounds in a solid-phase aqueous system was investigated with the aim of developing an environment-friendly and efficient derivatization method for HPLC analyses of environmental samples. The phenols were rapidly and efficiently converted to the tosyl derivatives on a commercially available ODS solid-phase cartridge by passing an aqueous buffer solution through it. The solid-phase aqueous tosylation system has been incorporated into a preconcentration step performed by solid-phase extraction from environmental water. |
| |
Keywords: | |
本文献已被 PubMed 等数据库收录! |
|