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Crystal and molecular structures of 2-(4-chlorophenyl)-5,7-dimethoxyquinolin-4-yl phenyl bis(2-chloroethyl) phosphoramidate
Authors:J. W. Yuan   L. B. Qu   X. L. Chen   Z. B. Qu  Y. C. Li
Affiliation:(1) Laboratoire de Structure, Elaboration et Applications des Mat?riaux Mol?culaires (SEA2M), D?partement de G?nie des Proc?d?s, Facult? des Sciences et de la Technologie, University of Mostaganem, 27000 Mostaganem, Algeria;(2) CNR-IC Institute of Crystallography, Via Amendola 122/O, 70126 Bari, Italy;(3) Laboratoire de Synth?se Organique Appliqu?e (LSOA), D?partement de Chimie, Facult? de Sciences, University of Oran–Es-S?nia, 31000 Oran, Algeria;;
Abstract:2-(4-Chlorophenyl)-5,7-dimethoxyquinolin-4-yl phenyl bis(2-chloroethyl)phosphoramidate is synthesized and characterized by NMR, IR and single crystal X-ray crystallography. The crystal is triclinic, P[`1]Pbar 1 space group, with a = 9.5188(19) ?, b = 12.856(3) ?, c = 13.250(3) ?, V = 1412.0(5) ?)3, and Z = 2 (at 291(2) K). The crystal packing arrangement indicates that the molecule is stacked through π...π aromatic stacking interactions.
Keywords:
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