| 1-苯甲酰-2-苯磺酰肼类化合物的合成 |
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| 引用本文： | 史海波.1-苯甲酰-2-苯磺酰肼类化合物的合成[J].合成化学,2007,15(3):372-373,393. |
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| 作者姓名： | 史海波 |
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| 作者单位： | 浙江医药高等专科学校,应用生物系,浙江,宁波,315100 |
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| 摘 要： | 以苯磺酰肼为原料,在低温下滴加苯甲酰氯,方便地合成了7个1-苯甲酰-2-苯磺酰肼类化合物,收率40.3%～75.8%。其结构经1H NMR表征。
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| 关 键 词： | 芳酰肼 芳磺酰肼 芳酰氯 合成 |
| 文章编号： | 1005-1511（2007）03-0372-02 |
| 收稿时间： | 2006-04-12 |
| 修稿时间： | 2006-04-122006-06-16 |
Synthesis of 1-Benzoyl-2-phenylsulfonyl-hydrazine Derivatives |
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| SHI Hai-bo.Synthesis of 1-Benzoyl-2-phenylsulfonyl-hydrazine Derivatives[J].Chinese Journal of Synthetic Chemistry,2007,15(3):372-373,393. |
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| Authors: | SHI Hai-bo |
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| Institution: | Department of Applied Biology, Zhejiang College of Pharmaceutical, Ningbo 315100, China |
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| Abstract: | Seven 1-benzoyl-2-phenylsulfonyl-hydrazine derivatives in yield of 40.3%~75.8% were facilely synthesized via reaction of phenylsulfonyl-hydrazine derivatives and substituted benzoyl chloride at low temperatures.Their structures were confirmed by 1H NMR. |
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| Keywords: | benzoylhydrazine phenylsulfonyl-hydrazine benzoyl chloride synthesis |
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