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A structural investigation of tris(ethyl acetoacetate)aluminium (III) |
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| Authors: | S Kurajica J Popović T Gazivoda Kraljević E Tkalčec I Simčić V Mandić A Altomare A Moliterni X Rocquefelte |
| Institution: | 1. Faculty of Chemical Engineering and Technology, University of Zagreb, 19 Maruli?ev trg, Zagreb, Croatia 2. Ru?er Bo?kovi? Institute, Bijeni?ka cesta 54, Zagreb, Croatia 3. Pliva Croatia Ltd., Prilaz baruna Filipovi?a 25, Zagreb, Croatia 4. Institute of Crystallography-CNR, Via Amendola 122/o, Bari, Italy 5. Institut des Matériaux Jean Rouxel, Université de Nantes, 2 rue de la Houssinière, 44322, Nantes, France |
| Abstract: | Aluminium tris(ethyl acetoacetate), Al(C6H9O3)3 has been prepared and characterized by means of 1H and 13C nuclear magnetic resonance spectroscopy, scanning electron microscopy and X-ray powder diffraction (XRPD). It was determined that two stereoisomeric complexes can be distinguished in the solution: meridional and facial. The crystal structure of Al(C6H9O3)3 has been determined from XRPD data. The compound crystallizes in the monoclinic space group P21/n. |
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