| 2-苯羟甲基-5,5-二甲基-4-苯基-2-氧代1,3,2-二氧磷杂环己烷的合成及表征 |
| |
| 引用本文： | 张想竹,吴明书,孙宝盛.2-苯羟甲基-5,5-二甲基-4-苯基-2-氧代1,3,2-二氧磷杂环己烷的合成及表征[J].应用化学,2007,24(1):114-0. |
| |
| 作者姓名： | 张想竹 吴明书 孙宝盛 |
| |
| 作者单位： | a天津大学环境科学与工程学院，天津 300072；b安阳工学院化工系，安阳 |
| |
| 摘 要： | 以苯甲醛、异丁醛、三氯化磷为原料合成了新型的1,3,2-二氧磷杂环类化合物2-苯羟甲基-5,5-二甲基-4-苯基-2-氧代-1,3,2-二氧磷杂环己烷,总收率为40．8％,并对其进行了NMR研究和结构表征。
|
| 关 键 词： | 二氧磷杂环己烷 合成 表征 |
| 文章编号： | 1000-0518(2007)01-0114-03 |
| 收稿时间： | 2009-06-29 |
| 修稿时间： | 2006-01-13 |
Synthesis and characterization of 2-( 1-Phenyl-1-hydroxy) methyl-5,5-dimethyl-4-phenyl-1,3,2-dioxaphosphorinane 2-oxide |
| |
| ZHANG Xiang-Zhu,Wu Ming-Shu,SUN Bao-Sheng.Synthesis and characterization of 2-( 1-Phenyl-1-hydroxy) methyl-5,5-dimethyl-4-phenyl-1,3,2-dioxaphosphorinane 2-oxide[J].Chinese Journal of Applied Chemistry,2007,24(1):114-0. |
| |
| Authors: | ZHANG Xiang-Zhu Wu Ming-Shu SUN Bao-Sheng |
| |
| Institution: | a School of Environmental Engineering, Tianjin University, Tanjin 300072 ; b Department of Chemical engineering,Anyang Institute of Technology,Anyang |
| |
| Abstract: | The novel title compound was synthesized with benzaldehyde, isobutyraldehyde, phosphorus trichloride as raw materials. The total yield was 40. 8%. The structure was confirmed by 1H NMR, 31P NMR and elemental analysis. |
| |
| Keywords: | synthesis dioxaphosphorinane oxide characterization |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
| 点击此处可从《应用化学》浏览原始摘要信息 |
| 点击此处可从《应用化学》下载免费的PDF全文 |
|
