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High-density MgB2 superconducting bulk samples prepared at ambient pressure
Authors:An Ling    Chen Chin-ping    Li Xing-guo   Feng Qing-rong
Affiliation:(1) School of Physics and State Key Laboratory for Mesoscopic Physics, Peking University, Beijing, 100871, China;(2) Department of Chemistry, Peking University, Beijing, 100871, China;(3) Department of Physics, Changji College, Changji, 831100, China
Abstract:High-density MgB2 (HD-MgB2) superconducting samples (D ⩾ 2.2 g/cm3), using different sources of magnesium powder as raw material, were synthesized in ambient pressure in a rich Mg environment. The magnesium powders used in the fabrication process include nanometer-sized magnesium particles, powders from Alfa Aesar, ordinary off-the-shelf powder, and magnesium chip. The fabrication procedure involved a double-sintering process in a rich-Mg environment. A transition temperature T c of 39 K was observed. Samples with the equally high density and matching superconducting properties were obtained as well by a triple sintering process of the MgB2 powder directly from Alfa Aesar.
Keywords:high-density MgB2 superconductor  magnesium vapor in all directions  sintering process
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