Crystal growth and characterization of K2B4O11H8 |
| |
| Authors: | Xingcheng Luo Shilie Pan Xiaoyun Fan Jide Wang Gang Liu |
| |
| Institution: | 1. College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046, China;2. Xinjiang Technical Institute of Physics & Chemistry, Chinese Academy of Sciences, 40-1 South Beijing Road, Urumqi, Xinjiang 830011, China |
| |
| Abstract: | Single crystals of K2B4O11H8, a non-centrosymmetric borate material, have been prepared by slow evaporation of water solution at room temperature. The crystals were colorless and transparent with smooth faces. The single-crystal X-ray diffraction analysis showed that K2B4O11H8 crystallized in the orthorhombic space group P212121 with a=6.8556(6) Å, b=11.7787(12) Å, c=12.8949(14) Å, Z=4, R1=0.0188, and wR2=0.0464. The powder X-ray diffractometry (PXRD), infrared spectrum, transmittance spectrum, TG–DTA curves and second harmonic generation properties of title compound have been determined. |
| |
| Keywords: | 61 66 Fn 81 10 Dn 42 65 Ky |
| 本文献已被 ScienceDirect 等数据库收录！ |
|
