Vortex grinding for mechanochemistry: application for automated supramolecular catalysis and preparation of a metal-organic framework |
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Authors: | Jelena Stojaković Brian S Farris Leonard R MacGillivray |
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Institution: | Department of Chemistry, University of Iowa, Iowa City, IA, USA. |
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Abstract: | An automated grinding method based on a vortex mixer has been developed. The method enables simultaneous grinding and UV-irradiation, as well as in situ monitoring of solid-state reactivity. The method has been applied to a cocrystallization, supramolecular catalysis, and the preparation of a metal-organic framework. |
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