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气相色谱/质谱法测定卷烟烟气中的主要挥发酸
引用本文:何爱民,苏国岁.气相色谱/质谱法测定卷烟烟气中的主要挥发酸[J].分析测试技术与仪器,2005,11(2):120-122.
作者姓名:何爱民  苏国岁
作者单位:石家庄卷烟厂技术中心,河北,石家庄,050051;石家庄卷烟厂技术中心,河北,石家庄,050051
摘    要:以异丙醇为溶剂,壬醇为内标,采用气相色谱/质谱法定性定量分析了卷烟烟气中的游离态甲酸和乙酸,还测定了该方法的精密度和准确度,结果为:RSD小于2%,回收率大于97%.

关 键 词:卷烟烟气  总粒相物  甲酸  乙酸  气相色谱/质谱法
文章编号:1006-3757(2005)02-0120-03
收稿时间:4/4/2005 12:00:00 AM
修稿时间:2005年4月4日

Determination of Main Volatile Acid in Cigarette Smoke by GC/MS
HE Ai-min and SU Guo-sui.Determination of Main Volatile Acid in Cigarette Smoke by GC/MS[J].Analysis and Testing Technology and Instruments,2005,11(2):120-122.
Authors:HE Ai-min and SU Guo-sui
Institution:Technical Center of Shijiazhuang Cigarette Factory, Shijiazhuang 050051, China;Technical Center of Shijiazhuang Cigarette Factory, Shijiazhuang 050051, China
Abstract:Using isopropyl alcohol as a solvent and n-nonanol as an internal standard, the content of free formic acid and free acetic acid in cigarette smoke was qualitatively and quantitatively determined by GC/MS. The precision and the accuracy of this method were also determined. RSD of the method was less than 2% and recovery was better than 97%.
Keywords:cigarette smoke  smoke condensates  formic acid  acetic acid  GC/MS
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