Zerstörungsfreie aktivierungsanalytische Bestimmung von Mikro- und Ultramikromengen Indium in Reinstthallium und Thalliumverbindungen |
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Authors: | Christo Daiev Stoyan Alexandrov Lilan Daieva |
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Institution: | 1. Chemische Fakult?t, Universit?t ?Kl. Ochridski“, Sofia, Bulgarien
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Abstract: | Two non-destructive neutron activation methods has been described for the determination of indium in thallium metal and thallium compounds. The sensitivity of the first method based on114mIn corresponds to 1×10?6g (standard deviation 4,5–8%). The second method (by means of116mIn) permits the determination of ultramicro amounts of indium up to 5×10?11g with a standard deviation of 15%. The influence of many elements (such as Ga, Cu, Al, Cd, Zn, Pb, Ca, Mg, Bi, Fe) has been examined. The methods have been applied to the determination of indium in thallium metal, oxide, nitrate, sulphate and chloride. The data obtained agreed whith those of the spectrochemical determination. |
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