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Synthesis of 5-nitrofuryl-2- and fury L-2-propiolic acid
Authors:K. K. Venter  S. P. Korshunov  L. I. Vereshchagin  R. L. Bol'shedvorskaya  D. O. Lolya  S. A. Giller
Affiliation:(1) Institute of Organic Synthesis AS Latvian SSR, Riga;(2) Institute of Petroleum and Carbochemical Synthesis, Zhdanov Irkutsk State University, USSR
Abstract:Nitration of methyl furyl-2-propiolate in acetic anhydride at -25° gives methyl 5-nitrofuryl-2-propiolate in good yield. Methods for preparing furyl-2-propiolic acid and its methyl ester are described.
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