| 研磨法合成1,2,3,6-四氢嘧啶-2-酮衍生物 |
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| 引用本文： | 靳通收,赵莹,刘利宾,李同双. 研磨法合成1,2,3,6-四氢嘧啶-2-酮衍生物[J]. 有机化学, 2006, 26(7): 975-978 |
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| 作者姓名： | 靳通收 赵莹 刘利宾 李同双 |
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| 作者单位： | 河北大学化学与环境科学学院,保定,071002 |
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| 摘 要： | 以NH2SO3H为催化剂, 室温无溶剂条件下, 研磨芳醛、β-酮酸酯和尿素合成了一系列1,2,3,6-四氢嘧啶-2-酮衍生物. 该方法具有反应条件温和、操作简便、环境友好、产率高等优点.
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| 关 键 词： | NH2SO3H 1,2,3,6-四氢嘧啶-2-酮 合成 研磨 |
| 收稿时间： | 2005-06-14 |
| 修稿时间： | 2006-01-18 |
Synthesis of 1,2,3,6-Tetrahydropyrimidin-2-one Derivatives by Grinding Method |
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| JIN Tong-Shou,ZHAO Ying,LIU Li-Bin,LI Tong-Shuang. Synthesis of 1,2,3,6-Tetrahydropyrimidin-2-one Derivatives by Grinding Method[J]. Chinese Journal of Organic Chemistry, 2006, 26(7): 975-978 |
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| Authors: | JIN Tong-Shou ZHAO Ying LIU Li-Bin LI Tong-Shuang |
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| Affiliation: | College of Chemistry and Environmental Science, Hebei University, Baoding 071002 |
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| Abstract: | NH2SO3H was used to efficiently perform one-pot, three-component, Biginelli condensation reactions of aldehydes, β-ketoesters and urea under solvent-free conditions at room temperature by grinding method. The method offered several advantages including mild reaction conditions, simple experimental procedure, environmental friendliness and excellent yield. |
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| Keywords: | aminosulfonic acid 1 2 3 6-tetrahydropyrimidin-2-one synthesis grinding method |
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