| 自旋回波技术在31P谱中的应用 |
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| 引用本文： | 翟纯. 自旋回波技术在31P谱中的应用[J]. 波谱学杂志, 1987, 4(2): 179-184 |
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| 作者姓名： | 翟纯 |
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| 作者单位： | 石油化工科学研究院 |
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| 摘 要： | 本文将自旋回波技术用于识别直接与31P核偶合(31P-1H)和远程偶合(31P-O-C-1H)的氢类型。例举了二烷基二硫代磷酸、二烷基磷酸酯及其他几种产物中自旋回波方法归属的结果。
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| 关 键 词： | 含磷脂类 自旋回波技术 31P NMR |
| 收稿时间： | 1986-10-22 |
APPLICATION OF SPIN-ECHO TECHNIQUE IN ~(31)P NMR SPECTROSCOPY |
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| Zhai Chun. APPLICATION OF SPIN-ECHO TECHNIQUE IN ~(31)P NMR SPECTROSCOPY[J]. Chinese Journal of Magnetic Resonance, 1987, 4(2): 179-184 |
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| Authors: | Zhai Chun |
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| Affiliation: | Research Institute of Petroleum Processing |
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| Abstract: | Intensity modulated 31P NMR spectra were obtained by using the pulse sequence in a FT-80A spectrometer. Spin-echo techque for signal assignment could be applied to systems with direct couplings ( 31P-1H ) and long-range couplings (31P-O-C-1H ) fragments. Some applications to the dialkyldithiophosphoric acids, dialkyl phosphonates and other phosphorus containing compounds are discussed. |
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| Keywords: | Phosphorus Containing compounds Spin-echo techniqus ~(31)PNMR |
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