| 含硫Schiff碱的合成及其抑菌活性 |
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| 引用本文： | 颜莉,赵吉寿.含硫Schiff碱的合成及其抑菌活性[J].合成化学,2010,18(1). |
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| 作者姓名： | 颜莉 赵吉寿 |
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| 作者单位： | 1. 云南民族大学,数学与计算机学院,云南,昆明,650031
2. 云南民族大学,化学与生物技术学院,云南,昆明,650031 |
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| 摘 要： | 1-苯基-3-甲基-4-苯甲酰基-5-吡唑啉酮分别与氨基硫脲、肼基二硫代甲酸苄酯、肼基二硫代甲酸甲酯和1,3-二氨基硫脲反应合成了6个含硫Schiff碱(6a~6 e),其结构经UV,1H NMR,IR和元素分析表征。初步生物活性测试结果表明,部分6对大肠杆菌和枯草芽孢杆菌具有一定的抑菌活性。
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| 关 键 词： | 吡唑啉酮 含硫Schiff碱 抑菌活性 合成 |
Synthesis and Fungicidal Activity of Schiff Bases Containing Sulfur |
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| YAN Li,ZHAO Ji-shou.Synthesis and Fungicidal Activity of Schiff Bases Containing Sulfur[J].Chinese Journal of Synthetic Chemistry,2010,18(1). |
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| Authors: | YAN Li ZHAO Ji-shou |
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| Abstract: | Six Schiff bases(6a～6e) containing sulfur were synthesized by the reaction of 1-phenyl-3-methyl-5-oxo-4-pyrazolone with aminothiourea,S-benzyldithiocarbazate,S-methyldithiocarbazate and 1,3-diaminothiourea,respectively.The structures were characterized by UV,~1H NMR,IR and elemental analysis.The results of preliminary biological activity tests showed that some of 6 exhibited some fungicidal activities to E.coli and Bacillus subtilis. |
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| Keywords: | pyrazolone sulphur-containing Schiff base fungicidal activity synthesis |
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