Synthesis of N-substituted 9-[2-(3,4-methylenedioxyphenyl)-2-oxoethyl]-1,5-dinitro-7,8-benzo-3-azabicyclo[3.3.1]non-7-en-6-ones |
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| Authors: | I. E. Yakunina Yu. M. Atroshchenko I. V. Shahkheldyan K. I. Kobrakov N. A. Troizkiy O. I. Boikova |
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| Affiliation: | (1) L. N. Tolstoi Tula State Pedagogical University, Tula, 300026, Russia;(2) A. N. Kosygin Moscow State Textile University, Moscow, 117918;(3) N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, 119991 |
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| Abstract: | Aminomethylation has been accomplished of the anionic Yanovskii adduct of 2,4-dinitronaphthol and 3,4-dimethylenedioxyacetophenone. The structure of the 3-substituted 9-[2-(3,4-methylenedioxyphenyl)-2-oxoethyl]-1,5-dinitro-7,8-benzo-3-azabicylo[3.3.1]non-7-en-6-one was determined by two-dimensional homo-and heteronuclear correlation spectroscopy. __________ Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 9, 1382–1389, September 2007. |
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| Keywords: | 3-azabicyclo[3.3.1]nonanes anionic Yanovskii adducts homo-and heteronuclear correlation spectroscopy aminomethylation reaction Mannich reaction |
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