烟用接装纸质控样品的制备与应用

采用深珠光印字烟用接装纸作为质控样品,用微波消解处理质控样品,以电感耦合等离子体质谱法(ICP–MS)对样品的铬、砷、铅含量进行定值,并进行不确定度评定。利用方差分析评价均匀性,ADF检验评价稳定性。经F检验表明在95%的置信区间,制备的烟用接装纸质控样品均匀性良好;经ADF检验表明,各元素在1%的显著水平下稳定可靠,样品稳定性良好。将烟用接装纸质控样品用于质控,并绘制Levy–Jennings质控图,质控效果良好。

Preparation and Application of a Quality Controlling Sample of the Tipping Paper for Cigarette

With deep pearl printing tipping paper as the cigarette of quality control sample, the chromium,arsenic, lead in the quality controlling samples were determined by inductively coupled plasma mass spectrometry （ICP-MS） with microwave digestion,and the uncertainty of the measurement results were evaluated. The analysis of variance was used to evaluate the homogeneity,the ADF-test was used to evaluate the stability. The analysis of variance showed that the results of sample were not different significantly in the 95%confidence interval,and were considered homogeneous. The ADF-test results showed that the elements were significant at 1%level,and were considered stable. The cigarette paper quality control samples were used for quality control, and map Levy-Jennings quality control, quality control effect was good.