Synthesis and absolute configuration of +-lineatin,the pheromone of |
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Authors: | Kenji Mori Tamon Uematsu Masao Minobe Kazunori Yanagi |
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Institution: | Department of Agricultural Chemistry, The University of Tokyo, Yayoi, 1-1-1, Bunkyo-ku, Tokyo 113 Japan;Central Research Laboratory, Sumitomo Chemical Co., Tsukahara 2–40, Takatsuki-shi, Osaka 569, Japan |
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Abstract: | A new synthesis of (±), (+)- and (-)-lineatin (3,3,7-trimethyl-2, 9-dioxatricyclo 3.3.1.04,7] nonane, ) was achieved. The stereochemistry of (+)-lineatin was established as 1, 4, 5, 7 by an X-ray crystallographic analysis of an intermediate . |
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