Synthesis of bastadin-6 trimethyl ether,a novel 28-membered ring lactam |
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| Authors: | Shigeru Nishiyama Tomoka Suzuki Shosuke Yamamura |
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| Institution: | Department of Chemistry, Faculty of Science and Technology, Keio University Hiyoshi, Yokohama, Japan |
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| Abstract: | Bastadin-6 trimethyl ether, a 28-membered ring lactam, was synthesized by means of phenolic exidation of dibromobastadin-2 trimethyl ether with thallium (III0 nitrate (TTN) leading to the formation of the corresponding macrocyclic biphenyl ether as a key step. From bastadin-2 trimethyl ether, a 26-membered ring compound was also synthesized. |
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