Dosage du plutonium dans les alliages plutonium aluminium par fluorescence-x |
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| Authors: | M Ganivet Th Arnal |
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| Institution: | Services des Elements Combustibles au Plutonium et d''Etudes Radiométallurgiques, Commissariat á I''Energie Atomique Centre d''Etudes Nucléaires de Cadarache France |
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| Abstract: | An X-ray fluorescence method is described for the determination of plutonium in Pu-Al alloys. In order to obtain satisfactory reproducibility, the alloy is first dissolved in a nitric acid-mercury (II) nitrate mixture. The Lα emission of plutonium is measured, to eliminate matrix effects, an internal standard with a wavelength near that of the Pu emission is used. Equipment and sample preparation are described. Extension of the method to other determinations is discussed. |
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