Determination of traces of hydrogen in fluoro-organic compounds |
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| Authors: | R. Belcher M.K. Bhatty A.M.G. Macdonald S.A. Salam J.C. Tatlow |
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| Affiliation: | Department of Chemistry, The University, BirminghamGreat Britain |
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| Abstract: | The determination of traces of hydrogen in highly fluorinated compounds has been studied. Nitrogen and sulphur in the sample interfere slightly in the pyrolytic method of Miller etal. A straightforward combustion method is proposed in which the sample is burned in oxygen over magnesium oxide at 900° and the water formed is determined either gravimetrically or titrimetrically. |
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