Nitrogen-tellurium-containing heterocycles. 4. X-ray structure of 2-phenylbenzotellurazole |
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Authors: | A. é. Mistryukov I. D. Sadekov V. S. Sergienko G. M. Abakarov M. A. Porai-Koshits A. A. Shneider A. D. Garnovskii |
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Affiliation: | (1) Scientific-Research Institute of Physical and Organic Chemistry, Rostov State University, 344104 Rostov-on-Don;(2) Institute of General and Inorganic Chemistry, Academy of Sciences of the USSR, 117021 Moscow |
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Abstract: | The crystal and molecular structure of 2-phenylbenzotellurazole is determined by x-ray methods. The heterocyclic fragment of the molecule is planar. The dihedral angle between planes of the heterocycle and the 2-phenyl substituent is 31.2. Somewhat shortened Te-N intermolecular ocntacts (3.43 å) are seen in the crystal. These do not substantially affect the physical properties of the compound.For Communication 3, see [1].Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 12, pp. 1690–1692, December, 1989. |
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