Structure of 6,13-bis(<Emphasis Type="Italic">N</Emphasis>, <Emphasis Type="Italic">N</Emphasis>-dimethylcarbamoyl) thioquinanthrene |
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Authors: | Email author" target="_blank">Andrzej?Ma?lankiewiczEmail author Ewa?Michalik Tadeusz?G?owiak Andrzej?Kowalski |
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Institution: | (1) Department of Organic Chemistry, The Medical University of Silesia Jagiello ska 4, 41-200, Sosnowiec, Poland;(2) Institute of Chemistry, University of Wroc aw, F.Joliot-Curie 14, 50-383, Wroc aw, Poland;(3) Oxford Diffraction, ul. Rogowska 127A, 54-440, Wroc aw, Poland |
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Abstract: | The crystal structure of 6,13-bis-(N,N-dimethylcarbamoyl)thioquinanthrene 3 has been determined as monoclinic, with space group P2(1)/c with lattice parameters a = 10.044(2) Å, b = 21.385(4) Å, c = 10.889(3) Å, = 102.92(3)°, Z = 4 and Dcalc = 1.342 Mg/m3. The middle 1,4-dithiin ring in the title compound 3, C24H20N4O2S2 is in a boat conformation with the dihedral angle between the planes of the aromatic rings 132.45(8)°. |
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Keywords: | 1 4-Dithiin ring dimethylcarbamoyl group quinoline derivatives |
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